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Redox Chemistry

Topic 4 of 6

Aqueous electrolysis: more than one possible ion

Water introduces competing products.

O-Level 6092 (2026) / SEC G3 K324 (2027)

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Aqueous electrolysis: more than one possible ion

Water introduces competing products.

In aqueous electrolysis, consider the solute ions and the water. With inert electrodes, a metal less reactive than hydrogen, such as copper, is usually deposited at the cathode. For a very reactive metal ion such as Na+, hydrogen forms instead. At the anode, sulfate is generally not discharged; oxygen forms from water/hydroxide. Halide concentration matters: concentrated chloride favours chlorine, while dilute chloride solution is treated here as giving oxygen.

Apply selective discharge to a new solution
  1. List species and electrode material

    For aqueous potassium iodide with inert electrodes, consider K+, I- and water (H+ and OH-). Molten KI has no water competing.

  2. Choose the cathode product

    Potassium is above hydrogen in the reactivity series. In the school aqueous model, hydrogen forms rather than potassium metal. For a metal below hydrogen, such as copper or silver, the metal is normally deposited.

  3. Choose the anode product

    Halide discharge forms the corresponding halogen: bromide gives bromine; iodide gives iodine. For this iodide solution iodine forms; 2I-(aq) -> I2(aq) + 2e-. Chloride needs the dilute/concentrated comparison shown below. Sulfate is not discharged in these examples: oxygen forms from water/hydroxide.

  4. Check atoms, charge and observations

    The iodide half-equation has two iodine atoms and total charge -2 on each side. The anode region becomes brown as iodine dissolves; hydrogen bubbles at the cathode. Do not describe every halogen product as a gas.

Predict products with inert electrodes
ElectrolyteCathodeAnode
Aqueous copper(II) sulfateCopperOxygen
Dilute aqueous sodium chlorideHydrogenOxygen
Concentrated aqueous sodium chlorideHydrogenChlorine
Useful balanced half-equations
ProcessHalf-equation
Copper depositionCu2+(aq) + 2e- -> Cu(s)
Hydrogen from water2H2O(l) + 2e- -> H2(g) + 2OH-(aq)
Oxygen from hydroxide4OH-(aq) -> O2(g) + 2H2O(l) + 4e-
Chlorine from chloride2Cl-(aq) -> Cl2(g) + 2e-

Worked example

Construct a half-equation from an unfamiliar ion charge

An aqueous solution contains Ag+ ions and silver is discharged at an inert cathode. A separate molten lead(II) bromide cell produces bromine at the anode. Construct the relevant half-equations.

  1. At the cathode an Ag+ ion gains one electron to make a neutral silver atom: Ag+(aq) + e- -> Ag(s).
  2. At the anode bromide ions lose electrons. Bromine is Br2, so begin 2Br- -> Br2, then add 2e- on the right to balance charge.
  3. For the molten-cell anode use Br-(l) and Br2(g); the molten electrolyte is hot enough for bromine to be a gas. Check both atoms and net charge.
Answer

Cathode in the silver solution: Ag+(aq) + e- -> Ag(s). Anode in molten lead(II) bromide: 2Br-(l) -> Br2(g) + 2e-. Each equation must balance atoms and charge.

Worked example

Compare dilute and concentrated brine

Explain why changing NaCl concentration can change one electrode product.

  1. Na+ is not deposited from either aqueous solution; hydrogen forms at the cathode.
  2. In dilute solution, oxygen forms at the inert anode.
  3. At high chloride concentration, chloride is preferentially discharged and chlorine forms.
Answer

Cathode product remains hydrogen; anode product changes. Always state aqueous/molten, concentration and electrode material.

Check your understandingWhat happens to the blue colour during electrolysis of copper(II) sulfate with inert electrodes?Think it through, then reveal the answer
It becomes paler as Cu2+ ions are removed at the cathode and are not replenished by an inert anode. Copper deposits and oxygen is produced.